C₂₂H₃₄O₄Si

Base Information

Chemical Name:C₂₂H₃₄O₄Si
CAS No.:1388152-92-8
Molecular Formula:C₂₂H₃₄O₄Si
Molecular Weight:390.595
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:

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Chemical Property of C₂₂H₃₄O₄Si

Chemical Property:

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Technology Process of C₂₂H₃₄O₄Si

There total 11 articles about C₂₂H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388153-27-2
C₂₁H₃₂O₅Si

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1388152-92-8
C₂₂H₃₄O₄Si

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

C₂₁H₃₂O₅Si; In tetrahydrofuran; at -78 - 0 ℃; for 2h;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388152-92-8
C₂₂H₃₄O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

With camphor-10-sulfonic acid; potassium tert-butylate; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-88-2
C₁₄H₂₀O₄

: 1388152-92-8
C₂₂H₃₄O₄Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

5.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

6.1: tetrahydrofuran / 0.83 h / 20 °C

7.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

9.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

10.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

11.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

11.2: 2 h / -78 - 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z