dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine

Base Information

Chemical Name:dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine
CAS No.:438000-80-7
Molecular Formula:C₅₂H₆₀N₄O₈Pd₂
Molecular Weight:1081.91
Hs Code.:

Synonyms:

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Chemical Property of dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine

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Technology Process of dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine

There total 2 articles about dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3375-31-3
palladium diacetate

: 3,6-bis(4'-(butyloxy)phenyl)pyridazine

: 438000-80-7,373387-81-6
bis(μ-acetato)bis[3,6-bis(4'-(butyloxy)phenyl)pyridazine]dipalladium

Guidance literature:: In acetic acid; addn. of Pd acetate (2.63E-4 mol) to soln. of the pyridazine (2.63E-4 mol) in acetic acid, heating at 60°C for 6 h; solvent was removed;
DOI:10.1021/om010449g

Reference yield: 100.0%

: 3375-31-3
palladium diacetate

: 3,6-bis(4'-(butyloxy)phenyl)pyridazine

: 373387-81-6,438000-80-7
dipalladium(μ-acetato)-3,6-bis(4'-butyloxyphenyl)pyridazine

Guidance literature:: In acetic acid; a soln. of pyridazine and Pd salt (1:1) in acetic acid heated at 60°C for 48 h; the solvent removed to yield a solid;
DOI:10.1016/S0022-328X(01)01330-4

Reference yield: 73.0%

: 438000-80-7,373387-81-6
bis(μ-acetato)bis[3,6-bis(4'-(butyloxy)phenyl)pyridazine]dipalladium

: 1118-67-8
sodium (Z)-4-oxopent-2-en-2-olate

: 373387-83-8
(acetylacetonate)[3,6-bis(4'-(butyloxy)phenyl)pyridazine]palladium

Guidance literature:: In acetone; addn. of Na acetylacetonate to soln. of the Pd complex in acetone, stirring at room temp. for 18 h; solvent was removed, chromy. (silica gel, CHCl3/CH3OH (90/10)); elem. anal.;
DOI:10.1021/om010449g