Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

Base Information

Chemical Name:Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)
CAS No.:70657-55-5
Molecular Formula:C₂₇H₂₀Fe₂NO₆P
Molecular Weight:597.127
Hs Code.:

Fe<sub>2</sub>(CO)6(CHCC<sub>6</sub>H<sub>5</sub>NHCH<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)2)

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Chemical Property of Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

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Technology Process of Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

There total 1 articles about Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 52970-25-9
diiron(CO)6(μ2-η2-CCPh)(μ-PPh2)

: 70657-55-5
Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

: 73970-08-8
Fe₂(CO)6(CHC₆H₅CNHCH₃)(P(C₆H₅)2)

Guidance literature:: With methylamine; In diethyl ether; a soln. of complex and a large excess of amine was stirred at room temp. for 10 min, N2 atm.; concn., column chromy. (Florisil, heptane/benzene), recrystn. (heptane,-70°C); elem. anal.;

Reference yield: 92.0%

: 70657-55-5
Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

: silver perchlorate

: 84280-70-6
Fe₂Ag(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)=Fe₂Ag(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)ClO₄

Guidance literature:: In benzene; Ag salt dissolved in a minimum of benzene adding to an equimolar amt. of Fe complex soln. with vigorous stirring under N2, after 5 min, ppt. allownig to settle, mother liquor removing by syringe or in vacuo, washingwith benzene and drying in vacuo; identified by elem. anal., IR, NMR, Moessbauer spectra and single crystal X-ray diffraction;

Reference yield: 90.0%

: 26042-63-7
silver(I) hexafluorophosphate

: 70657-55-5
Fe₂(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)

: 84280-79-5
Fe₂Ag(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)⁽¹⁺⁾*PF₆^(1-)=Fe₂Ag(CO)6(CHCC₆H₅NHCH₃)(P(C₆H₅)2)PF₆

Guidance literature:: In tetrahydrofuran; benzene; Ag salt dissolved in THF adding to an equimolar amt. of Fe complex soln. in benzene with vigorous stirring under N2, after 5 min, ppt. allownigto settle, mother liquor removing by syringe or in vacuo, washing with benzene and drying in vacuo; identified by elem. anal., IR, NMR and Moessbauer spectra;