resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate

Base Information

Chemical Name:resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate
CAS No.:315667-11-9
Molecular Formula:C₃₂H₂₃F₃O₄P₂Pd
Molecular Weight:696.895
Hs Code.:

Synonyms:

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Chemical Property of resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate

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Technology Process of resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate

There total 1 articles about resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: palladium(II) trifluoroacetate

: 279214-81-2
1,3-bis(diphenylphosphinito)benzene

: 315667-11-9
Pd(CH((C(OP(C₆H₅)2)CH)2CH))(OC(O)CF₃)

Guidance literature:: In tetrahydrofuran; under N2; soln. of Pd(OCOCF3)2 and resorcinolbis(diphenyl)phosphinite (1:1 mol) in THF stirred at room temp. 2 h; evapd. (vac.); residue washed (EtOH); crystd. (CH2Cl2-EtOH); elem. anal.;
DOI:10.1039/b004793g

Reference yield:

: 315667-11-9
resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate

: 1730-25-2
allylmagnesium bromide

: 714271-70-2
[((C₆H₅)2POC₆H₃OP(C₆H₅)2)Pd(CH₂CHCH₂)]

Guidance literature:: In tetrahydrofuran-d8; soln. of CH2CHCH2MgBr in THF-d8 was added to soln. of Pd complex in THF-d8 at -10°C; NMR monitoring; not isolated;
DOI:10.1021/ja049357j

Reference yield:

: 315667-11-9
resorcinolbis[(diphenyl)phosphinite] palladium trifluoroacetate

: 762-73-2
trimethyl(allyl)stannane

: 714271-70-2
[((C₆H₅)2POC₆H₃OP(C₆H₅)2)Pd(CH₂CHCH₂)]

Guidance literature:: In tetrahydrofuran-d8; byproducts: Me3SnOCOCF3; CH2CHCH2SnMe3 was added to soln. of Pd complex in THF-d8 at -10°C; NMR monitoring; not isolated;
DOI:10.1021/ja049357j