BF₂(3,5-bis(trifluoromethyl)phenyl)

Base Information

• Chemical Name: BF₂(3,5-bis(trifluoromethyl)phenyl)
• CAS No.: 1372168-75-6
• Molecular Formula: C₈H₃BF₈
• Molecular Weight: 261.91
• Mol file: 1372168-75-6.mol

Synonyms:

Chemical Property of BF₂(3,5-bis(trifluoromethyl)phenyl)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BF₂(3,5-bis(trifluoromethyl)phenyl)

There total 1 articles about BF₂(3,5-bis(trifluoromethyl)phenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

boron trifluoride (7637-07-2) + SnMe3(C6H3(CF3)2-3,5) (17197-30-7) → BF2(3,5-bis(trifluoromethyl)phenyl) (1372168-75-6)

Guidance literature:

In hexane; at 60 ℃; for 18h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1002/chem.201301056

Reference yield: 38.0%

bis(tricyclohexylphosphine)platinum(0) (55664-33-0) + Na[B(3,5-bis(trichloromethyl)phenyl)4] + BF2(3,5-bis(trifluoromethyl)phenyl) (1372168-75-6) → trans-[[Pt(BF(3,5-bis(trifluoromethyl)phenyl))](PCy3)2][B(3,5-bis(trichloromethyl)phenyl)4]

Guidance literature:

In fluorobenzene; hexane; at 20 ℃; for 0.25h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1002/chem.201301056

Reference yield: 37.0%

bis(tricyclohexylphosphine)platinum(0) (55664-33-0) + BF2(3,5-bis(trifluoromethyl)phenyl) (1372168-75-6) → trans-[(Cy3P)2Pt-BF2(3,5-bis(trifluoromethyl)phenyl)]

Guidance literature:

In hexane; benzene-d6; at 20 ℃; for 6h; Schlenk technique; Inert atmosphere; Glovebox;

DOI:10.1002/chem.201301056

upstream raw materials:

boron trifluoride

SnMe₃(C₆H₃(CF₃)2-3,5)

Downstream raw materials:

ethylenebis(tricyclohexylphosphine)platinum