C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-)
• CAS No.: 1426316-61-1
• Molecular Formula: Br*C₃₆H₄₉NPS₂
• Molecular Weight: 670.802
• Mol file: 1426316-61-1.mol

Synonyms:

Chemical Property of C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-)

There total 1 articles about C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + (3-bromopropyl)tributylphosphonium bromide (918895-51-9) + 10-benzyl-9,10-dihydroacridine (87742-33-4) → C36H49NPS2(1+)*Br(1-) (1426316-61-1)

Guidance literature:

10-benzyl-9,10-dihydroacridine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; hexane; Inert atmosphere;

(3-bromopropyl)tributylphosphonium bromide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; Inert atmosphere;

DOI:10.1021/ja312039k

Reference yield:

C36H49NPS2(1+)*Br(1-) (1426316-61-1) + 6-bromohexanoic acid N-hydroxysuccinimide ester (42014-54-0) → C46H62N2O4PS2(1+)*Br(1-) (1242242-37-0)

Guidance literature:

C₃₆H₄₉NPS₂⁽¹⁺⁾*Br^(1-); With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;

6-bromohexanoic acid N-hydroxysuccinimide ester; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;

DOI:10.1021/ja312039k

upstream raw materials:

carbon disulfide

(3-bromopropyl)tributylphosphonium bromide

10-benzyl-9,10-dihydroacridine

Downstream raw materials:

C₄₆H₆₂N₂O₄PS₂⁽¹⁺⁾*Br^(1-)