PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)={PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)}ClO₄

Base Information

• Chemical Name: PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)={PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)}ClO₄
• CAS No.: 155113-82-9
• Molecular Formula: C₃₂H₃₁ClNP₂Pt*ClO₄
• Molecular Weight: 821.536

Synonyms:

Chemical Property of PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)={PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)}ClO₄

Chemical Property:

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Safty Information:

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Useful:

Technology Process of PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)={PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)}ClO₄

There total 1 articles about PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)⁽¹⁺⁾*ClO₄^(1-)={PtCl(C₅H₄NCH₃)(P(C₆H₅)2C₂H₄P(C₆H₅)2)}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.2%

sodium perchlorate monohydrate (7791-07-3) + PtCl(1,2-bis(diphenylphosphino)ethane)(C5H4N-C(2)) + dimethyl sulfate (77-78-1) → PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)(1+)*ClO4(1-)={PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)}ClO4 (155113-82-9)

Guidance literature:

In benzene; addn. of dimethyl sulfate to soln. of Pt compd. in benzene, standing overnight at room temp.; concn. in vac., diln. (Et2O), pptn., filtered off, redissolved in CH2Cl2, treated with NaClO4*H2O in MeOH, evapn. in vac., extn. (CH2Cl2 and charcaol), filtration, addn. of MeOH, evapn. of CH2Cl2 in vac., pptn., further re-pptn.; elem. anal.;

DOI:10.1039/DT9940000407

Reference yield: 64.8%

sodium perchlorate monohydrate (7791-07-3) + PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)(1+)*ClO4(1-)={PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)}ClO4 (155113-82-9) + p-methoxyphenylisonitrile (10349-38-9) → Pt(CNC6H4OCH3)(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)(2+)*2ClO4(1-)={Pt(CNC6H4OCH3)(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)}(ClO4)2

Guidance literature:

In dichloromethane; soln. of Pt compd. in CH2Cl2 treated with the isocyanide, after 10 min addn. of NaClO4*H2O dissolved in MeOH; evapn. in vac., extn. (CH2Cl2 and charcaol), filtration, addn. of MeOH, evapn. of CH2Cl2 in vac., pptn., further repptn.; elem. anal.;

DOI:10.1039/DT9940000407

Reference yield:

PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)(1+)*ClO4(1-)={PtCl(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)}ClO4 (155113-82-9) + p-methoxyphenylisonitrile (10349-38-9) → Pt(C(NHC6H4OCH3)2)(C5H4NCH3)(P(C6H5)2C2H4P(C6H5)2)(2+)*2ClO4(1-)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: chloroform

In dichloromethane; chloroform;

DOI:10.1039/DT9940000407

upstream raw materials:

sodium perchlorate monohydrate

dimethyl sulfate

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