Linolenic acid ketone

Base Information

• Chemical Name: Linolenic acid ketone
• CAS No.: 1169768-30-2
• Molecular Formula: C₃₇H₆₆O
• Molecular Weight: 526.93
• Mol file: 1169768-30-2.mol

Synonyms:

Chemical Property of Linolenic acid ketone

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Linolenic acid ketone

There total 9 articles about Linolenic acid ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-ol (1169768-28-8) → dilinoleyl ketone (1169768-30-2)

Guidance literature:

With sodium carbonate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1.75h;

Reference yield: 82.0%

(6Z,9Z,28Z,31Z)-19-nitroheptatriaconta-6,9,28,31-tetraene → dilinoleyl ketone (1169768-30-2)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 4h; Temperature; Reagent/catalyst;

Reference yield: 74.0%

(Z,Z)-octadeca-9,12-dienyl bromide (4102-60-7,13044-37-6) + (10Z,13Z)-10,13-nonadecadienenitrile → dilinoleyl ketone (1169768-30-2)

Guidance literature:

(Z,Z)-octadeca-9,12-dienyl bromide; With magnesium; In diethyl ether; at 35 ℃; for 1h; Inert atmosphere; Reflux;

(10Z,13Z)-10,13-nonadecadienenitrile; In diethyl ether; at 20 ℃;

With sulfuric acid; In water;

upstream raw materials:

(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-ol

(Z,Z)-octadeca-9,12-dienyl bromide

(9Z,12Z)-octadeca-9,12-dienyl methanesulfonate

(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-yl formate

Downstream raw materials:

2,2-dilinoleyl-4-(2-dimethylaminoethyl)-[1,3]-dioxolane