<1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch...

Base Information

• Chemical Name: <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch...
• CAS No.: 92998-15-7
• Molecular Formula: C₁₄₄H₁₈₄Br₃Cl₂O₃₀P₃
• Molecular Weight: 2798.57

Synonyms:

Chemical Property of <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch...

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Technology Process of <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch...

There total 1 articles about <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(benzotriazol-1-yl)(2-chlorophenyl)phosphate (80817-46-5) + 1,2-di-O-stearoyl-3-O-<6-O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl>-sn-glycerol (81692-29-7) + 2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol (92982-69-9) → <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch... (92998-15-7)

Guidance literature:

With 1-methyl-1H-imidazole; Yield given. Multistep reaction; 1.) oxolane, 20 deg C, 45 min, 2.) oxolane, 1.5 h;

DOI:10.1016/0008-6215(84)85277-5

Reference yield: 82.0%

triethylammonium hydrogencarbonate + <1,2-di-O-stearoyl-sn-glycer-3-yl O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside>-<(6->3)-2-chlorophenylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-ch... (92998-15-7) → C142H183Cl2O30P3*C6H15N (92982-71-3)

Guidance literature:

With pyridine; 2,4,6-tri(iso-propyl)benzenesulfonic acid; acetylacetone; zinc; for 0.0833333h;

DOI:10.1016/0008-6215(84)85277-5

upstream raw materials:

bis(benzotriazol-1-yl)(2-chlorophenyl)phosphate

1,2-di-O-stearoyl-3-O-<6-O-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-β-D-glucopyranosyl>-sn-glycerol

2-O-benzyl-sn-glycerol-<(1->3)-2,2,2-tribromoethylphospho>-2-O-benzyl-sn-glycerol-<(1->3)-2-chlorophenylphospho>-1,2-di-O-benzyl-sn-glycerol

Downstream raw materials:

C₁₄₂H₁₈₃Cl₂O₃₀P₃*C₆H₁₅N

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