C₁₀H₉F₂NO₂

Base Information

Chemical Name:C₁₀H₉F₂NO₂
CAS No.:1429939-91-2
Molecular Formula:C₁₀H₉F₂NO₂
Molecular Weight:213.184
Hs Code.:

C<sub>10</sub>H<sub>9</sub>F<sub>2</sub>NO<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₀H₉F₂NO₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₀H₉F₂NO₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₀H₉F₂NO₂

There total 1 articles about C₁₀H₉F₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5308-63-4
1-(5-methyl-pyridin-2-yl)-ethanone

: 454-31-9
ethyl difluoroacetate

: 1429939-91-2
C₁₀H₉F₂NO₂

Guidance literature:: 1-(5-methyl-pyridin-2-yl)-ethanone; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

ethyl difluoroacetate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ml400071a

Reference yield:

: 1429939-91-2
C₁₀H₉F₂NO₂

: 1429939-77-4
C₂₁H₂₀F₃N₅O

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 110 °C

2: sodium tetrahydroborate / ethanol / 3 h / Reflux

3: potassium hydroxide / water; ethanol / 80 °C

4: Resolution of racemate

5: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With sodium tetrahydroborate; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400071a