2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

Base Information

Chemical Name:2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine
CAS No.:131088-74-9
Molecular Formula:C₃₈H₅₁N₃O₁₁
Molecular Weight:725.836
Hs Code.:

2,3-di-O-benzyl-1-N-<N-(tert-butoxycarbonyl)-L-aspart-1-oyl-(L-proline methyl ester)-4-oyl>-4,6-O-isopropylidene-α-D-glucopyranosylamine

Synonyms:

Suppliers and Price of 2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

There total 8 articles about 2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 131088-76-1
N-(tert-butoxycarbonyl)-L-aspartyl-L-proline methyl ester

: 131088-74-9,131176-17-5
2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-β-D-glucopyranosylamine

: 131088-74-9,131176-17-5
2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; for 8h; Ambient temperature;
DOI:10.1016/0008-6215(90)80006-O

Reference yield: 41.0%

: 131088-76-1
N-(tert-butoxycarbonyl)-L-aspartyl-L-proline methyl ester

: 131088-74-9,131176-17-5
2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-β-D-glucopyranosylamine

: 131088-74-9,131176-17-5
2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; for 8h; Ambient temperature;
DOI:10.1016/0008-6215(90)80006-O

Reference yield:

: 30925-18-9
2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

: 131088-74-9,131176-17-5
2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / triethylamine, diethylcyanophosphonate / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

2: 88 percent / H₂ / 10percent Pd-C / ethanol / 12 h / Ambient temperature

3: 41 percent / triethylamine, diethyl cyanophosphonate / tetrahydrofuran / 8 h / Ambient temperature

With diethyl cyanophosphonate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80006-O