C₂₆H₃₄N₄OPSe⁽¹⁺⁾*BF₄^(1-)

Base Information

• Chemical Name: C₂₆H₃₄N₄OPSe⁽¹⁺⁾*BF₄^(1-)
• CAS No.: 1542136-76-4
• Molecular Formula: BF₄*C₂₆H₃₄N₄OPSe
• Molecular Weight: 615.321
• Mol file: 1542136-76-4.mol

Synonyms:

Chemical Property of C₂₆H₃₄N₄OPSe⁽¹⁺⁾*BF₄^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₂₆H₃₄N₄OPSe⁽¹⁺⁾*BF₄^(1-)

There total 3 articles about C₂₆H₃₄N₄OPSe⁽¹⁺⁾*BF₄^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H34N4OP(1+)*BF4(1-) (1542136-74-2) → C26H34N4OPSe(1+)*BF4(1-) (1542136-76-4)

Guidance literature:

With selenium; In toluene; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om4011577

Reference yield:

(1S,2S)-N1,N2-dibenzylcyclohexane-1,2-diamine (191480-61-2) → C26H34N4OPSe(1+)*BF4(1-) (1542136-76-4)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine; phosphorus trichloride / toluene / 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: triethylamine / toluene; acetonitrile; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

3: selenium / toluene / 24 h / 20 °C / Inert atmosphere; Schlenk technique

With selenium; triethylamine; phosphorus trichloride; In tetrahydrofuran; toluene; acetonitrile;

DOI:10.1021/om4011577

Reference yield:

(3aS,7aS)-1,3-Dibenzyl-2-chloro-octahydro-benzo[1,3,2]diazaphosphole → C26H34N4OPSe(1+)*BF4(1-) (1542136-76-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / toluene; acetonitrile; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

2: selenium / toluene / 24 h / 20 °C / Inert atmosphere; Schlenk technique

With selenium; triethylamine; In tetrahydrofuran; toluene; acetonitrile;

DOI:10.1021/om4011577

upstream raw materials:

(1S,2S)-N¹,N²-dibenzylcyclohexane-1,2-diamine

C₂₆H₃₄N₄OP⁽¹⁺⁾*BF₄^(1-)