C₁₅H₁₃ClN₂O₃

Base Information

• Chemical Name: C₁₅H₁₃ClN₂O₃
• CAS No.: 1261563-79-4
• Molecular Formula: C₁₅H₁₃ClN₂O₃
• Molecular Weight: 304.733
• Mol file: 1261563-79-4.mol

Synonyms:

Chemical Property of C₁₅H₁₃ClN₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₃ClN₂O₃

There total 3 articles about C₁₅H₁₃ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2,5-dimethoxy-aniline (6358-64-1) → C15H13ClN2O3 (1261563-79-4)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl acetamide / 120 °C

2: 10% palladium on activated charcoal; hydrogen

With 10% palladium on activated charcoal; hydrogen; potassium carbonate; In N,N-dimethyl acetamide;

DOI:10.1016/j.bmcl.2010.10.010

Reference yield:

C14H13ClN2O4 (1261563-66-9) → C15H13ClN2O3 (1261563-79-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 10% palladium on activated charcoal; hydrogen

With 10% palladium on activated charcoal; hydrogen;

DOI:10.1016/j.bmcl.2010.10.010

Reference yield:

phosgene (75-44-5) + C14H15ClN2O2 (1152563-48-8) → C15H13ClN2O3 (1261563-79-4)

Guidance literature:

phosgene; C₁₄H₁₅ClN₂O₂;

With boron tribromide;

DOI:10.1016/j.bmcl.2010.10.010

upstream raw materials:

phosgene

C₁₄H₁₅ClN₂O₂

C₁₄H₁₃ClN₂O₄

4-chloro-2,5-dimethoxy-aniline

Downstream raw materials:

C₁₃H₉ClN₂O₃