Technology Process of C16H20O3
There total 3 articles about C16H20O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium hydroxide; benzyltrimethylammonium chloride / methanol; dichloromethane / -20 - 20 °C
With
oxalyl dichloride; benzyltrimethylammonium chloride; dimethyl sulfoxide; sodium hydroxide;
In
methanol; dichloromethane;
1.1: |Swern Oxidation / 1.2: |Swern Oxidation;
DOI:10.1039/c3ob41020j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / dichloromethane / 24 h / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: sodium hydroxide; benzyltrimethylammonium chloride / methanol; dichloromethane / -20 - 20 °C
With
pyridine; oxalyl dichloride; benzyltrimethylammonium chloride; dimethyl sulfoxide; sodium hydroxide;
In
methanol; dichloromethane;
2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1039/c3ob41020j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / dichloromethane / 24 h / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: sodium hydroxide; benzyltrimethylammonium chloride / methanol; dichloromethane / -20 - 20 °C
With
pyridine; oxalyl dichloride; benzyltrimethylammonium chloride; dimethyl sulfoxide; sodium hydroxide;
In
methanol; dichloromethane;
2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1039/c3ob41020j