UDP-L-Ara

Base Information

Chemical Name:UDP-L-Ara
CAS No.:110222-42-9
Molecular Formula:C₁₄H₂₂N₂O₁₆P₂
Molecular Weight:536.28
Hs Code.:

Synonyms:

Suppliers and Price of UDP-L-Ara

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of UDP-L-Ara

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of UDP-L-Ara

There total 4 articles about UDP-L-Ara which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: uridine 5'-diphosphate-tetrabutyl ammonium

: (2R,3R,4S,5S)-2-Iodo-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran

: 15839-78-8,21401-20-7,30329-30-7,38-57-3,97905-92-5,7164-64-9
UDP-β-L-Arap

: 110222-42-9,21401-20-7,30329-30-7,38-57-3,97905-92-5,7164-64-9
UDP-L-Ara

Guidance literature:: uridine 5'-diphosphate-tetrabutyl ammonium; (2R,3R,4S,5S)-2-Iodo-3,4,5-tris-trimethylsilanyloxy-tetrahydro-pyran; In dichloromethane; for 4h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; for 1h;

With alkaline phosphatase; at 20 ℃; for 16h; pH=8; Title compound not separated from byproducts;
DOI:10.1080/07328309808001892

Reference yield:

: 87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2
L-(+)-arabinose

: 110222-42-9,21401-20-7,30329-30-7,38-57-3,97905-92-5,7164-64-9
UDP-L-Ara

Guidance literature:: Multi-step reaction with 3 steps

1.1: 100 percent / pyridine / 1 h / 0 °C

2.1: iodotrimethylsilane / CH₂Cl₂ / 0.5 h / 20 °C

3.1: CH₂Cl₂ / 4 h

3.2: tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran / 1 h

3.3: alkaline phosphatase / various solvent(s) / 16 h / 20 °C / pH 8

With pyridine; trimethylsilyl iodide; In dichloromethane; 1.1: Substitution / 2.1: Substitution / 3.1: Substitution / 3.2: Hydrolysis / 3.3: Hydrolysis;
DOI:10.1080/07328309808001892

Reference yield:

: 32166-73-7
per-O-trimethylsilyl-L-arabinose

: 110222-42-9,21401-20-7,30329-30-7,38-57-3,97905-92-5,7164-64-9
UDP-L-Ara

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodotrimethylsilane / CH₂Cl₂ / 0.5 h / 20 °C

2.1: CH₂Cl₂ / 4 h

2.2: tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran / 1 h

2.3: alkaline phosphatase / various solvent(s) / 16 h / 20 °C / pH 8

With trimethylsilyl iodide; In dichloromethane; 1.1: Substitution / 2.1: Substitution / 2.2: Hydrolysis / 2.3: Hydrolysis;
DOI:10.1080/07328309808001892