2-Chloro-5-hydrazinobenzoic acid hydrochloride

Base Information

• Chemical Name: 2-Chloro-5-hydrazinobenzoic acid hydrochloride
• CAS No.: 184163-49-3
• Molecular Formula: C₇H₇ClN₂O₂*ClH
• Molecular Weight: 223.059
• European Community (EC) Number: 867-905-8

Synonyms:2-chloro-5-hydrazinobenzoic acid hydrochloride;184163-49-3;2-chloro-5-hydrazinylbenzoic acid hydrochloride;2-chloro-5-hydrazinylbenzoic acid;hydrochloride;SCHEMBL6697133;LYSZNCNDYFXUJI-UHFFFAOYSA-N;AKOS000103213;DB-192717;2-chloro-5-hydrazinylbenzoicacidhydrochloride;CS-0219262;EN300-03551;5-Hydrazino-2-chlorobenzoic acid hydrochloride;G28642

Chemical Property of 2-Chloro-5-hydrazinobenzoic acid hydrochloride

Chemical Property:

• Vapor Pressure: 2.68E-07mmHg at 25°C
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 221.9962829
• Heavy Atom Count: 13
• Complexity: 177

Purity/Quality:

98%Min ^*data from raw suppliers

2-chloro-5-hydrazinylbenzoicAcidHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=C(C=C1NN)C(=O)O)Cl.Cl

Technology Process of 2-Chloro-5-hydrazinobenzoic acid hydrochloride

There total 3 articles about 2-Chloro-5-hydrazinobenzoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-chloro-5-aminobenzoic acid (89-54-3) → 2-chloro-5-hydrazinobenzoic acid hydrochloride (184163-49-3)

Guidance literature:

2-chloro-5-aminobenzoic acid; With hydrogenchloride; sodium nitrate; for 0.5h; cooling;

With hydrogenchloride; tin(ll) chloride; at 5 ℃; for 1h;

DOI:10.1016/S0968-0896(03)00183-4

Reference yield: 71.0%

C7H4ClN2O2(1+)*Cl(1-) (24569-37-7) → 2-chloro-5-hydrazinobenzoic acid hydrochloride (184163-49-3)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In water; at 5 - 10 ℃; for 1h;

Reference yield:

SnCl2 *2H2 O + 2-chloro-5-aminobenzoic acid (89-54-3) → 2-chloro-5-hydrazinobenzoic acid hydrochloride (184163-49-3)

Guidance literature:

With sodium nitrite; In hydrogenchloride; water;

upstream raw materials:

2-chloro-5-aminobenzoic acid

C₇H₄ClN₂O₂⁽¹⁺⁾*Cl^(1-)

Downstream raw materials:

6-chloro-2,3,4,9-tetrahydro-1H-carbazole-7-carboxylic acid

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