C₄₇H₅₈F₂N₈O₆

Base Information

Chemical Name:C₄₇H₅₈F₂N₈O₆
CAS No.:1419384-78-3
Molecular Formula:C₄₇H₅₈F₂N₈O₆
Molecular Weight:869.024
Hs Code.:

C<sub>47</sub>H<sub>58</sub>F<sub>2</sub>N<sub>8</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₄₇H₅₈F₂N₈O₆

Chemical Property:

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Technology Process of C₄₇H₅₈F₂N₈O₆

There total 18 articles about C₄₇H₅₈F₂N₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007882-04-3
(S)-tert-butyl 2-(5-(4-bromophenyl)-1H-imidazol-2-yl)pyrrolidine-1-carboxylate

: 1419384-78-3
C₄₇H₅₈F₂N₈O₆

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / ethyl acetate / 20 °C

2: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

5: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1419384-78-3
C₄₇H₅₈F₂N₈O₆

Guidance literature:: Multi-step reaction with 6 steps

1: ammonia / methanol / 0 - 20 °C

2: N-iodo-succinimide / dichloromethane / 1.5 h / 0 °C

3: sodium sulfite / ethanol; water / 17 h / Reflux

4: hydrogenchloride / ethyl acetate / 0 - 20 °C

5: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0 - 20 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

With hydrogenchloride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; potassium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium sulfite; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 13336-31-7
4-methoxylindanone

: 1419384-78-3
C₄₇H₅₈F₂N₈O₆

Guidance literature:: Multi-step reaction with 9 steps

1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice

2: Lawessons reagent / toluene / 18 h / Inert atmosphere; Reflux

3: antimony(III) chloride; (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 18 h / 20 °C / Inert atmosphere; Cooling with ice

4: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 20 °C / Cooling with ice

5: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

6: pyridine / dichloromethane / 3.33 h / 20 °C / Inert atmosphere; Cooling with ice

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

8: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 100 °C / Inert atmosphere

9: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

With Lawessons reagent; pyridine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium tert-butylate; potassium acetate; antimony(III) chloride; boron tribromide; potassium carbonate; trifluoroacetic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;