1-phenethyl-piperidine-3-carboxylic acid pyrrolidide

Base Information

• Chemical Name: 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide
• CAS No.: 101715-40-6
• Molecular Formula: C₁₈H₂₆N₂O
• Molecular Weight: 286.417
• Mol file: 101715-40-6.mol

Synonyms:

Chemical Property of 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide

There total 2 articles about 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nicotinic acid (59-67-6) → 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide (101715-40-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂; chlorocarbonic acid ethyl ester; triethylamine

2: methanol / Hydrieren des Reaktionsprodukts an Platin in H₂O oder Aethanol

With methanol; dichloromethane; chloroformic acid ethyl ester; triethylamine;

DOI:10.1021/ja01512a051

Reference yield:

(pyridin-3-yl)(pyrrolidin-1-yl)methanone (77727-88-9) + 1-phenyl-2-bromoethane (103-63-9) → 1-phenethyl-piperidine-3-carboxylic acid pyrrolidide (101715-40-6)

Guidance literature:

With methanol; Hydrieren des Reaktionsprodukts an Platin in H₂O oder Aethanol;

DOI:10.1021/ja01512a051

upstream raw materials:

(pyridin-3-yl)(pyrrolidin-1-yl)methanone

1-phenyl-2-bromoethane

nicotinic acid