cis-anti-cis-10-phenylperhydroacridine

Base Information

• Chemical Name: cis-anti-cis-10-phenylperhydroacridine
• CAS No.: 114544-13-7
• Molecular Formula: C₁₉H₂₇N
• Molecular Weight: 269.43

Synonyms:

Chemical Property of cis-anti-cis-10-phenylperhydroacridine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of cis-anti-cis-10-phenylperhydroacridine

There total 3 articles about cis-anti-cis-10-phenylperhydroacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-phenyl-sym-octahydroacridinium perchlorate → cis-syn-cis-10-phenylperhydroacridine (114544-16-0) + cis-anti-cis-10-phenylperhydroacridine (30382-37-7,30426-05-2,42885-32-5,114544-13-7,114544-16-0)

Guidance literature:

With hydrogen; aniline; nickel ruthenium; In ethanol; at 100 ℃; under 75006 Torr; Title compound not separated from byproducts;

DOI:10.1007/BF02256983

Reference yield:

nitrobenzene (98-95-3,26969-40-4) + bis(2-oxocyclohexyl)methane (3137-39-1) → cis-syn-cis-10-phenylperhydroacridine (114544-16-0) + cis-anti-cis-10-phenylperhydroacridine (30382-37-7,30426-05-2,42885-32-5,114544-13-7,114544-16-0)

Guidance literature:

With hydrogen; ruthenium-modified Raney Ni; In methanol; at 100 ℃; under 75006 Torr; Yield given. Yields of byproduct given;

DOI:10.1007/BF00534272

Reference yield:

racem. 2,2'-methanediyl-bis-cyclohexanone (3137-39-1,6556-83-8,6556-85-0,30469-93-3) + aniline (62-53-3) → cis-syn-cis-10-phenylperhydroacridine (114544-16-0) + cis-anti-cis-10-phenylperhydroacridine (30382-37-7,30426-05-2,42885-32-5,114544-13-7,114544-16-0)

Guidance literature:

With hydrogen; Raney NI/Ru; Title compound not separated from byproducts;

DOI:10.1007/BF00472257

upstream raw materials:

nitrobenzene

bis(2-oxocyclohexyl)methane

racem. 2,2'-methanediyl-bis-cyclohexanone

aniline

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