zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin

Base Information

• Chemical Name: zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin
• CAS No.: 128703-42-4
• Molecular Formula: C₅₆H₄₄Br₈N₄Zn
• Molecular Weight: 1477.61
• Mol file: 128703-42-4.mol

Synonyms:

Chemical Property of zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin

There total 1 articles about zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N-Bromosuccinimide (128-08-5) + (tetrakis(2,4,6-trimethylphenyl)porphyrinato)zinc(II) (104025-54-9) → zinc(II) 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetramesitylporphyrin (128703-42-4)

Guidance literature:

In methanol; heating soln. of Zn-compound to reflux; slowly addn. of NBS; heating period 1h; cooling in an ice bath; filtration; purifn. by chromy.; collecting green fraction; evapn. to dryness; monitoring by UV-spectroscopy;

upstream raw materials:

N-Bromosuccinimide

(tetrakis(2,4,6-trimethylphenyl)porphyrinato)zinc(II)