N-[(Dibutylamino)methyl]methacrylamide

Base Information

Chemical Name:N-[(Dibutylamino)methyl]methacrylamide
CAS No.:92168-48-4
Molecular Formula:C13H26 N2 O
Molecular Weight:226.362
Hs Code.:
European Community (EC) Number:295-902-6
DSSTox Substance ID:DTXSID60238908
Nikkaji Number:J333.376K
Wikidata:Q83121250
Mol file:92168-48-4.mol

Synonyms:EINECS 295-902-6;92168-48-4;N-[(DIBUTYLAMINO)METHYL]METHACRYLAMIDE;N-((Dibutylamino)methyl)methacrylamide;SCHEMBL3282459;DTXSID60238908;N-(di-n-butylaminomethyl)methacrylamide;N-[(Dibutylamino)methyl]-2-methylpropenamide

Suppliers and Price of N-[(Dibutylamino)methyl]methacrylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N-[(Dibutylamino)methyl]methacrylamide

Chemical Property:

Vapor Pressure:3.62E-05mmHg at 25°C
Boiling Point:353.3°Cat760mmHg
Flash Point:167.5°C
PSA：35.83000
Density:0.901g/cm³
LogP:3.37870
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:226.204513457
Heavy Atom Count:16
Complexity:206

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN(CCCC)CNC(=O)C(=C)C

Technology Process of N-[(Dibutylamino)methyl]methacrylamide

There total 5 articles about N-[(Dibutylamino)methyl]methacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 67953-77-9
N-(hydroxymethyl)dibutylamine

: 79-39-0
Methacrylamide

: 92168-48-4
N-[(dibutylamino)methyl]-2-methylprop-2-enamide

Guidance literature:: With hydroquinone; In water; at 30 ℃; for 8h;

Reference yield: 69.0%

: 80179-56-2
N,N-dibutylmethaniminium chloride

: 79-39-0
Methacrylamide

: 92168-48-4
N-[(dibutylamino)methyl]-2-methylprop-2-enamide

Guidance literature:: N,N-dibutylmethaniminium chloride; Methacrylamide; In acetonitrile; at 20 ℃; for 3h;

With sodium carbonate; In water; for 0.5h;
DOI:10.1039/c8ob00811f

Reference yield:

: 111-92-2
dibutylamine

: 92168-48-4
N-[(dibutylamino)methyl]-2-methylprop-2-enamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 0 - 20 °C

2.1: acetyl chloride / diethyl ether / 1 h / 0 °C

3.1: acetonitrile / 3 h / 20 °C

3.2: 0.5 h

With acetyl chloride; In diethyl ether; acetonitrile;
DOI:10.1039/c8ob00811f