cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole

Base Information

• Chemical Name: cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole
• CAS No.: 96814-45-8
• Molecular Formula: C₁₈H₁₇N₃O
• Molecular Weight: 291.352

Synonyms:

Chemical Property of cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole

Chemical Property:

Purity/Quality:

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Technology Process of cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole

There total 9 articles about cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

semicarbazide hydrochloride (563-41-7) + 2-benzylidene-1-tetralone (6261-32-1) → trans-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9) + cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9)

Guidance literature:

With hydrogenchloride; In ethanol; for 2h; Heating;

Reference yield: 80.0%

semicarbazide hydrochloride (563-41-7) + 2-benzylidene-1-tetralone (6261-32-1) → trans-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9) + cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9)

Guidance literature:

With hydrogenchloride; In ethanol; for 2h; Heating;

Reference yield: 55.0%

(E)-2-benzylidene-1-tetralone (6261-32-1) + hydrazine carboxamide (4426-72-6,51433-48-8,57-56-7) → trans-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9) + cis-2-carbamoyl-3-phenyl-3,3a,4,5-tetrahydro-2H-benzindazole (96814-45-8,96814-46-9)

Guidance literature:

With potassium hydroxide; In ethanol; at 70 - 80 ℃;

DOI:10.1016/j.saa.2014.06.134

upstream raw materials:

semicarbazide hydrochloride

2-benzylidene-1-tetralone

(E)-2-benzylidene-1-benzosuberone

hydrazine carboxamide

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