Technology Process of 4-Benzyloxy-3-(2-hydroxy-phenyl)-butane-1,2-diol
There total 6 articles about 4-Benzyloxy-3-(2-hydroxy-phenyl)-butane-1,2-diol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; sodium metabisulphide;
In
pyridine; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature
2: potassium carbonate / acetone / 16 h / Heating
3: 72 percent / neat (no solvent) / 0.5 h / Heating
4: osmium tetraoxide, sodium metabisulphide / pyridine; H2O
With
osmium(VIII) oxide; sodium metabisulphide; phosphorus tribromide; potassium carbonate;
In
pyridine; diethyl ether; water; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 65 percent / lithium aluminium hydride / tetrahydrofuran
2: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature
3: potassium carbonate / acetone / 16 h / Heating
4: 72 percent / neat (no solvent) / 0.5 h / Heating
5: osmium tetraoxide, sodium metabisulphide / pyridine; H2O
With
osmium(VIII) oxide; lithium aluminium tetrahydride; sodium metabisulphide; phosphorus tribromide; potassium carbonate;
In
tetrahydrofuran; pyridine; diethyl ether; water; acetone;