Technology Process of C25H29N3O3S
There total 17 articles about C25H29N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran
2: thionyl chloride / toluene
3: N-ethyl-N,N-diisopropylamine / acetonitrile
4: water; sodium hydroxide / ethanol
With
thionyl chloride; tetrabutyl ammonium fluoride; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 8 steps
1: PhMe2NBr3
2: sodium diformamide
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
4: Lawessons reagent; pyridine / toluene / 100 °C
5: tetrabutyl ammonium fluoride / tetrahydrofuran
6: thionyl chloride / toluene
7: N-ethyl-N,N-diisopropylamine / acetonitrile
8: water; sodium hydroxide / ethanol
With
Lawessons reagent; pyridine; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 12 steps
1: sodium tetrahydroborate
2: 1H-imidazole
3: 3-chloro-benzenecarboperoxoic acid / ethanol
4: ethylmagnesium bromide / diethyl ether
5: diisobutylaluminium hydride / toluene
6: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene
7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
8: Lawessons reagent; pyridine / toluene / 100 °C
9: tetrabutyl ammonium fluoride / tetrahydrofuran
10: thionyl chloride / toluene
11: N-ethyl-N,N-diisopropylamine / acetonitrile
12: water; sodium hydroxide / ethanol
With
Lawessons reagent; pyridine; 1H-imidazole; sodium chlorite; sodium tetrahydroborate; potassium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; ethylmagnesium bromide; tetrabutyl ammonium fluoride; water; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067