trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

Base Information

Chemical Name:trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine
CAS No.:64982-81-6
Molecular Formula:C₂₂H₂₇NO₄
Molecular Weight:369.461
Hs Code.:

trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenz<c,g>azecine

Synonyms:

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Chemical Property of trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

Chemical Property:

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Technology Process of trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

There total 1 articles about trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64982-77-0,64982-79-2
2,3,11,12-Tetramethoxy-7-methyl-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolinium; chloride

: 64982-81-6
trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

: 78081-69-3
3-(4,5-Dimethoxy-2-vinyl-phenyl)-5,6-dimethoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given; 1.) water, IRA-400 resin, 2.) 95 deg C, 0.5 h;
DOI:10.1039/P19810001273

Reference yield:

: 64982-81-6
trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

: 65022-58-4
N-(2-formyl-3,4-dimethoxybenzyl)-N-(2-formyl-4,5-dimethoxyphenethyl)methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1N hydrochloric acid, N-bromosuccinimide, 2.) 3N sodium hydroxide

2: 280 mg / 1N sulphuric acid, periodic acid / H₂O / 0.17 h

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; sulfuric acid; periodic acid; In water;
DOI:10.1039/P19810001273

Reference yield:

: 64982-81-6
trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-cis-alpinigenine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1N hydrochloric acid, N-bromosuccinimide, 2.) 3N sodium hydroxide

2: 280 mg / 1N sulphuric acid, periodic acid / H₂O / 0.17 h

3: 30 percent / 2-methyl-propan-2-ol / 3.5 h / 37 °C / Irradiation

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; sulfuric acid; periodic acid; In water; tert-butyl alcohol;
DOI:10.1039/P19810001273