C₄H₃SC(O)Ge(C₆H₅)3

Base Information

Chemical Name:C₄H₃SC(O)Ge(C₆H₅)3
CAS No.:170307-10-5
Molecular Formula:C₂₃H₁₈GeOS
Molecular Weight:415.051
Hs Code.:

C<sub>4</sub>H<sub>3</sub>SC(O)Ge(C<sub>6</sub>H<sub>5</sub>)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄H₃SC(O)Ge(C₆H₅)3

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Technology Process of C₄H₃SC(O)Ge(C₆H₅)3

There total 1 articles about C₄H₃SC(O)Ge(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 98-03-3
thiophene-2-carbaldehyde

: 3839-32-5
triphenyl germyllithium

: 170307-10-5
C₄H₃SC(O)Ge(C₆H₅)3

Guidance literature:: With hydrogenchloride; In diethyl ether; N2; Ge-compd. soln. addn. to Ge-compd. soln. at 20°C, stirring 2 h, hydrolysis (HCl), extn., drying (Na2SO4), concn. under reduced pressure; residue treating with ether/pentane, pptn. after 12 h at -30°C, decantation and drying; elem. anal.;

Reference yield: 91.0%

: 3839-32-5
triphenyl germyllithium

: 170307-10-5
C₄H₃SC(O)Ge(C₆H₅)3

: 170307-08-1
C₄H₃SCH(OH)Ge(C₆H₂(CH₃)3)2H

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; N2; Al-compd. soln. (Et2O) addn. to Ge-compd. soln. (THF) at 0°C,hydrolysis (HCl) after 1 h at 0°C and 1 h at 20°C, extn., drying (Na2SO4), concn. under reduced pressure; residue treating with CH2Cl2 and than with pentane, pptn. after 12 h at -30°C, decantation and drying; elem. anal.;