(E)-β-(3,5-dimethylphenyl)vinyl bromide

Base Information

• Chemical Name: (E)-β-(3,5-dimethylphenyl)vinyl bromide
• CAS No.: 77385-75-2
• Molecular Formula: C₁₀H₁₁Br
• Molecular Weight: 211.101
• Mol file: 77385-75-2.mol

Synonyms:

Chemical Property of (E)-β-(3,5-dimethylphenyl)vinyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (E)-β-(3,5-dimethylphenyl)vinyl bromide

There total 2 articles about (E)-β-(3,5-dimethylphenyl)vinyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-Dimethyl-zimtsaeure (64781-23-3) → (E)-β-(3,5-dimethylphenyl)vinyl bromide (77385-75-2)

Guidance literature:

With N-Bromosuccinimide; lithium acetate; In water; acetonitrile; at 80 ℃; Inert atmosphere; Microwave irradiation;

DOI:10.1021/acs.orglett.1c03278

Reference yield:

3,5-dimethylstyrene (5379-20-4) → (E)-β-(3,5-dimethylphenyl)vinyl bromide (77385-75-2) + α-(3,5-dimethylphenyl)vinyl bromide (77385-74-1)

Guidance literature:

With potassium tert-butylate; bromine; Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/ja00400a047

upstream raw materials:

3,5-dimethylstyrene

3,5-Dimethyl-zimtsaeure