C₄₈H₆₄F₃NO₉S

Base Information

Chemical Name:C₄₈H₆₄F₃NO₉S
CAS No.:115560-01-5
Molecular Formula:C₄₈H₆₄F₃NO₉S
Molecular Weight:888.099
Hs Code.:

C<sub>48</sub>H<sub>64</sub>F<sub>3</sub>NO<sub>9</sub>S

Synonyms:

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Chemical Property of C₄₈H₆₄F₃NO₉S

Chemical Property:

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Technology Process of C₄₈H₆₄F₃NO₉S

There total 10 articles about C₄₈H₆₄F₃NO₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 115560-00-4
cholesteryl 4,6-O-benzylidene-3-O-(N-phenylcarbamoyl)-β-D-glucopyranoside

: 115560-01-5
C₄₈H₆₄F₃NO₉S

Guidance literature:: With pyridine; In dichloromethane; at -15 ℃; for 3h;
DOI:10.1016/S0008-6215(00)90561-5

Reference yield:

: 34368-66-6
1,2-O-isopropylidene-3-O-phenylcarbamoyl-α-D-glucofuranose

: 115560-01-5
C₄₈H₆₄F₃NO₉S

Guidance literature:: Multi-step reaction with 7 steps

1: 87 percent / 0.05 M H₂SO₄ / dioxane / 5 h / 100 °C

2: 93 percent / pyridine, 4-dimethylaminopyridine / 5 h / Ambient temperature

3: 82 percent / 33 percent HBr-AcOH / CHCl₃ / 5.5 h / Ambient temperature

4: 34 percent / silver 4-hydroxy valerate / diethyl ether / 6 h / Ambient temperature

5: K₂CO₃ / methanol / 4.5 h / Ambient temperature

6: 54 percent HBF₄ / dimethylformamide; diethyl ether / 27 h / Ambient temperature

7: pyridine / CH₂Cl₂ / 3 h / -15 °C

With pyridine; dmap; tetrafluoroboric acid; sulfuric acid; hydrogen bromide; Silber-4-hydroxy-valerat; potassium carbonate; acetic acid; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90561-5

Reference yield:

: 103-71-9
phenyl isocyanate

: 115560-01-5
C₄₈H₆₄F₃NO₉S

Guidance literature:: Multi-step reaction with 9 steps

1: 92 percent / 4-dimethylaminopyridine / toluene / 3 h / 100 °C

2: aq. acetic acid

3: 87 percent / 0.05 M H₂SO₄ / dioxane / 5 h / 100 °C

4: 93 percent / pyridine, 4-dimethylaminopyridine / 5 h / Ambient temperature

5: 82 percent / 33 percent HBr-AcOH / CHCl₃ / 5.5 h / Ambient temperature

6: 34 percent / silver 4-hydroxy valerate / diethyl ether / 6 h / Ambient temperature

7: K₂CO₃ / methanol / 4.5 h / Ambient temperature

8: 54 percent HBF₄ / dimethylformamide; diethyl ether / 27 h / Ambient temperature

9: pyridine / CH₂Cl₂ / 3 h / -15 °C

With pyridine; dmap; tetrafluoroboric acid; sulfuric acid; hydrogen bromide; Silber-4-hydroxy-valerat; potassium carbonate; acetic acid; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0008-6215(00)90561-5