sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

Base Information

Chemical Name:sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}
CAS No.:142040-07-1
Molecular Formula:C₁₄H₁₃BCoO₂*Na
Molecular Weight:306.05
Hs Code.:

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Chemical Property of sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

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Technology Process of sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

There total 1 articles about sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142040-05-9
di-μ-carbonyl-dicarbonylbis{η5-(3,4-dimethyl-1-phenylborol)}dicobalt(Co-Co)

: 142040-07-1
sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

Guidance literature:: With sodium amalgame; In dichloromethane; N2 atmosphere; stirring at -30°C for 2 h; filtration of excess amalgame; not isolated, detected by IR spectroscopy;

Reference yield: 64.0%

: 142040-07-1
sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

: 142040-14-0
dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))methylcobalt

Guidance literature:: With methyl iodide; In tetrahydrofuran; N2 atmosphere; addn. of MeI to soln. of Co-compd. in THF at -40°C, stirring at -40°C for 4 h; removal of solvent at -30°C under vac., addn. of Et2O, filtration at -30°C through kieselgur, partial evapn., layering with pentane, cooling at -70°C;

Reference yield:

: 33100-27-5
15-crown-5

: 142040-07-1
sodium {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

: 142040-12-8
{({15}-crown-5)sodium} {dicarbonyl-(η5-(3,4-dimethyl-1-phenylborol))cobaltate}

Guidance literature:: In tetrahydrofuran; N2 atmosphere; addn. of crown ether to soln. of Co-compd. in THF, stirring at room temp. for 10 min; removal of solvent (vac.), stirring with Et2O for 10 h, filtration, drying (vac.); elem. anal.;