N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

Base Information

Chemical Name:N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester
CAS No.:15889-52-8
Molecular Formula:C₄₀H₅₅N₉O₁₀S₂
Molecular Weight:886.063
Hs Code.:

N<sup>α</sup>-Carbobenzoxy-N<sup>G</sup>-tosyl-Arg-N<sup>G</sup>-tosyl-Arg-δ-amino-valeriansaeuremethylester

Synonyms:

Suppliers and Price of N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

Chemical Property:

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Technology Process of N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

There total 4 articles about N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63984-02-1
methyl 5-aminovalerate

: 15889-52-8
N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine / acetonitrile

2: Pd / (i) H₂, MeOH, (ii) /BRN= 2714107/, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine, Et₃N, acetonitrile

With 2-ethyl-5-phenylisoxazolium-3'-sulphonate; triethylamine; palladium; In acetonitrile;
DOI:10.1021/jo01268a060

Reference yield:

: 13650-38-9
N^α-Benzyloxycarbonyl-N^ω-tosyl-L-arginin

: 15889-52-8
N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine / acetonitrile

2: Pd / (i) H₂, MeOH, (ii) /BRN= 2714107/, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine, Et₃N, acetonitrile

With 2-ethyl-5-phenylisoxazolium-3'-sulphonate; triethylamine; palladium; In acetonitrile;
DOI:10.1021/jo01268a060

Reference yield:

: 627-95-2
5-amino-valeric acid ; hydrochloride

: 15889-52-8
N^α-Carbobenzoxy-N^G-tosyl-Arg-N^G-tosyl-Arg-δ-amino-valeriansaeuremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HCl

2: Et₃N, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine / acetonitrile

3: Pd / (i) H₂, MeOH, (ii) /BRN= 2714107/, 2-ethyl-5-<3-sulfo-phenyl>-isoxazolium betaine, Et₃N, acetonitrile

With hydrogenchloride; 2-ethyl-5-phenylisoxazolium-3'-sulphonate; triethylamine; palladium; In acetonitrile;
DOI:10.1021/jo01268a060