chloro(2-methyl-1-thioxopropylthio)diphenyltin

Base Information

Chemical Name:chloro(2-methyl-1-thioxopropylthio)diphenyltin
CAS No.:178534-58-2
Molecular Formula:C₁₆H₁₇ClS₂Sn
Molecular Weight:427.606
Hs Code.:

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Chemical Property of chloro(2-methyl-1-thioxopropylthio)diphenyltin

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Technology Process of chloro(2-methyl-1-thioxopropylthio)diphenyltin

There total 1 articles about chloro(2-methyl-1-thioxopropylthio)diphenyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 35329-04-5
2-methylpropanedithioic acid

: 1135-99-5
diphenyltin(IV) dichloride

: 178534-58-2
chloro(2-methyl-1-thioxopropylthio)diphenyltin

Guidance literature:: With triethylamine; In tetrahydrofuran; addn. of NEt3 to the acid in THF at -30°C, stirring (30 min), addn. of SnCl2Ph2 in THF, strring (-30°C, 1 h, room temp., 4 h); diln. with CHCl3 and H2O, extn. of the aq. phase with CHCl3, washing theorg. layer with H2O, drying (Na2SO4), concn. in vacuo, crystn. by addn. of a small amt. of acetone; elem. anal.;
DOI:10.1002/cber.19961290612