C₂₁H₃₄OSn

Base Information

Chemical Name:C₂₁H₃₄OSn
CAS No.:1357181-67-9
Molecular Formula:C₂₁H₃₄OSn
Molecular Weight:421.21
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₄OSn

Chemical Property:

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Technology Process of C₂₁H₃₄OSn

There total 1 articles about C₂₁H₃₄OSn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 688-73-3
tri-n-butyl-tin hydride

: 63697-96-1
4-Ethynylbenzaldehyde

: 1357181-67-9
C₂₁H₃₄OSn

: 4-(1-(tributylstannyl)vinyl)benzaldehyde

Guidance literature:: tri-n-butyl-tin hydride; With Cp*Fe(1,2-Ph₂PC₆H₄NH); In toluene; at 20 ℃; for 0.0333333h; Inert atmosphere;

4-Ethynylbenzaldehyde; In toluene; at 20 ℃; for 0.25h; Overall yield = 88 percent; Overall yield = 74.1 mg; regioselective reaction; Inert atmosphere;
DOI:10.1021/jacs.0c11448

Reference yield: 54.0%

: 1357181-67-9
C₂₁H₃₄OSn

: 124515-97-5
benzene

: (E)-(4-formylstyryl)phenyliodonium tosylate

Guidance literature:: In dichloromethane; 2,2,2-trifluoroethanol; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01705

Reference yield:

: 1357181-64-6
(Z)-ethyl 2-iodo-4-(4-methylphenylsulfonamido)-4-oxobut-2-enoate

: 1357181-67-9
C₂₁H₃₄OSn

: 1357181-52-2
4-ethoxycarbonyl-6-(4-formylphenyl)-1-(p-toluenesulfonyl)-1,6-dihydropyridin-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 1 h / 80 °C

2: o-xylene / 4 h / 130 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In 1,4-dioxane; o-xylene; 1: Migita-Stille coupling;
DOI:10.1016/j.tetlet.2011.12.014