Technology Process of C19H18N4O4
There total 11 articles about C19H18N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetic acid / acetonitrile / 0.25 h
2: potassium permanganate / water / 1.5 h / 80 °C
3: hydrogenchloride / water / 1 h / Reflux
4: triethylamine
5: potassium carbonate / acetone / 7 h / Reflux
6: 3-chloro-benzenecarboperoxoic acid / nitromethane; water / Inert atmosphere
7: Reflux
With
hydrogenchloride; potassium permanganate; potassium carbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
nitromethane; water; acetone; acetonitrile;
DOI:10.1002/jhet.1669
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / water / 1 h / Reflux
2: triethylamine
3: potassium carbonate / acetone / 7 h / Reflux
4: 3-chloro-benzenecarboperoxoic acid / nitromethane; water / Inert atmosphere
5: Reflux
With
hydrogenchloride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
nitromethane; water; acetone;
DOI:10.1002/jhet.1669
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium permanganate / water / 1.5 h / 80 °C
2: hydrogenchloride / water / 1 h / Reflux
3: triethylamine
4: potassium carbonate / acetone / 7 h / Reflux
5: 3-chloro-benzenecarboperoxoic acid / nitromethane; water / Inert atmosphere
6: Reflux
With
hydrogenchloride; potassium permanganate; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
nitromethane; water; acetone;
DOI:10.1002/jhet.1669