C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

Base Information

Chemical Name:C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂
CAS No.:133872-35-2
Molecular Formula:C₂₆H₁₈Br₂N₃S₂
Molecular Weight:604.325
Hs Code.:

C<sub>26</sub>H<sub>10</sub><sup>(2)</sup>H<sub>8</sub>Br<sub>2</sub>N<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

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Technology Process of C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

There total 6 articles about C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4165-57-5
bromobenzene-d5

: 133872-35-2
C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / chlorosulfonic acid / CHCl₃ / 1) 1 h, 0 deg C, 2) 1 h, reflux

2: 67 percent / zinc, sulfuric acid / H₂O / 12 h / Heating

3: Cl₂ / CH₂Cl₂

4: 79 percent / Et₃N / diethyl ether / 1 h / 0 °C

5: benzene / Ambient temperature; Irradiation

With chlorosulfonic acid; sulfuric acid; chlorine; triethylamine; zinc; In diethyl ether; dichloromethane; chloroform; water; benzene;
DOI:10.1021/jo00012a032

Reference yield:

: 133886-90-5
4-bromobenzenesulfenyl-d₄ chloride

: 133872-35-2
C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / diethyl ether / 1 h / 0 °C

2: benzene / Ambient temperature; Irradiation

With triethylamine; In diethyl ether; benzene;
DOI:10.1021/jo00012a032

Reference yield:

: 133872-23-8
4-bromobenzenesulfonyl-d₄ chloride

: 133872-35-2
C₂₆H₁₀⁽²⁾H₈Br₂N₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / zinc, sulfuric acid / H₂O / 12 h / Heating

2: Cl₂ / CH₂Cl₂

3: 79 percent / Et₃N / diethyl ether / 1 h / 0 °C

4: benzene / Ambient temperature; Irradiation

With sulfuric acid; chlorine; triethylamine; zinc; In diethyl ether; dichloromethane; water; benzene;
DOI:10.1021/jo00012a032