1-(2-Phenylprop-2-en-1-yl)naphthalene

Base Information

• Chemical Name: 1-(2-Phenylprop-2-en-1-yl)naphthalene
• CAS No.: 131061-07-9
• Molecular Formula: C19H16
• Molecular Weight: 244.336
• DSSTox Substance ID: DTXSID90564045
• Wikidata: Q82448624
• Mol file: 131061-07-9.mol

Synonyms:131061-07-9;1-(2-Phenylprop-2-en-1-yl)naphthalene;DTXSID90564045

Chemical Property of 1-(2-Phenylprop-2-en-1-yl)naphthalene

Chemical Property:

• XLogP3: 6.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 244.125200510
• Heavy Atom Count: 19
• Complexity: 297

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=C(CC1=CC=CC2=CC=CC=C21)C3=CC=CC=C3

Technology Process of 1-(2-Phenylprop-2-en-1-yl)naphthalene

There total 4 articles about 1-(2-Phenylprop-2-en-1-yl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

1-Naphthalenesulfonyl chloride (85-46-1) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → 1-(2-Phenyl-allyl)-naphthalene (131061-07-9) + 1-(2-phenyl-1-propenyl)-(E)-naphthalene (131061-06-8)

Guidance literature:

With potassium carbonate; benzyltrioctylammonium chloride; bis(benzonitrile)palladium(II) dichloride; In m-xylene; at 140 ℃; for 4h;

Reference yield: 50.0%

1-allylnaphthalene (2489-86-3) + phenylmagnesium bromide (100-58-3) → 1-(2-Phenyl-allyl)-naphthalene (131061-07-9)

Guidance literature:

With bis(acetylacetonate)nickel(II); N,N,N,N,-tetramethylethylenediamine; In toluene; at 20 ℃; for 12h; stereospecific reaction; Inert atmosphere;

DOI:10.1002/ejoc.201600955

Reference yield:

1-Bromonaphthalene (90-11-9) + isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) → 1-(2-Phenyl-allyl)-naphthalene (131061-07-9)

Guidance literature:

With palladium diacetate; potassium carbonate; 2-diphenylphosphino-2'-methylbiphenyl; In N,N-dimethyl-formamide; at 135 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.07.052

upstream raw materials:

1-Naphthalenesulfonyl chloride

isopropenylbenzene

1-Bromonaphthalene

iodobenzene