VINYLDIPHENYLMETHYLSILANE

Base Information

• Chemical Name: VINYLDIPHENYLMETHYLSILANE
• CAS No.: 13107-13-6
• Molecular Formula: C15H16Si
• Molecular Weight: 224.378
• Mol file: 13107-13-6.mol

Synonyms:Methyl-diphenyl-vinyl-silane;ethenylmethyldiphenyl-silane;VINYLDIPHENYLMETHYLSILANE;Silane, ethenylmethyldiphenyl-;diphenylmethylvinylsilane;

Chemical Property of VINYLDIPHENYLMETHYLSILANE

Chemical Property:

• Refractive Index: 0.997
• Boiling Point: 155 °C (12 mmHg)
• Flash Point: 125°C (257°F)
• PSA: 0.00000
• LogP: 2.60460

Purity/Quality:

98%,99%, ^*data from raw suppliers

VINYLDIPHENYLMETHYLSILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of VINYLDIPHENYLMETHYLSILANE

There total 10 articles about VINYLDIPHENYLMETHYLSILANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyllithium (917-54-4) → methyldiphenylvinylsilane (13107-13-6)

Guidance literature:

In tetrahydrofuran; at -78 ℃;

DOI:10.1246/cl.1994.231

Reference yield: 89.0%

methyl magnesium iodide (917-64-6) + (dibromomethyl)methyldiphenylsilane (102979-03-3) → methyldiphenylvinylsilane (13107-13-6)

Guidance literature:

methyl magnesium iodide; With manganese(ll) chloride; In tetrahydrofuran;

(dibromomethyl)methyldiphenylsilane; In tetrahydrofuran; at 25 ℃; for 2h;

DOI:10.1246/bcsj.73.2139

Reference yield: 89.0%

(dibromomethyl)methyldiphenylsilane (102979-03-3) → methyldiphenylvinylsilane (13107-13-6)

Guidance literature:

In tetrahydrofuran; at 25 ℃;

DOI:10.1016/S0040-4039(97)00601-1

upstream raw materials:

Dichloromethylvinylsilane

vinyldiphenylmethoxysilane

methylmagnesium bromide

dimethyl-[2-(methyl-diphenyl-silanyl)-ethyl]-amine

Downstream raw materials:

1--2--aethan

1,2-bis[diphenyl(methyl)silyl]ethane

1--2--aethan

octahydro-2,2′-bifuran