C₆₃H₆₄ClN₈O₁₆P

Base Information

Chemical Name:C₆₃H₆₄ClN₈O₁₆P
CAS No.:83327-01-9
Molecular Formula:C₆₃H₆₄ClN₈O₁₆P
Molecular Weight:1255.67
Hs Code.:

C<sub>63</sub>H<sub>64</sub>ClN<sub>8</sub>O<sub>16</sub>P

Synonyms:

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Chemical Property of C₆₃H₆₄ClN₈O₁₆P

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Technology Process of C₆₃H₆₄ClN₈O₁₆P

There total 13 articles about C₆₃H₆₄ClN₈O₁₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40608-06-8
levulinic anhydride

: 83327-01-9
C₆₃H₆₄ClN₈O₁₆P

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, 4-dimethylaminopyridine / diethyl ether; pyridine / Ambient temperature

2: 1.6 g / tetra-n-butylammonium flouride / tetrahydrofuran / 0.5 h

3: 2.) 2,4,6-triisopropylbenzenesulfonyl chloride / 1.) N-methylimidazole / 2.) pyridine, 30 min

With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride; triethylamine; 1-methyl-1H-imidazole; In tetrahydrofuran; pyridine; diethyl ether;
DOI:10.1016/0040-4020(84)85098-X

Reference yield:

: 961-07-9
2'-Deoxyguanosine

: 83327-01-9
C₆₃H₆₄ClN₈O₁₆P

Guidance literature:: Multi-step reaction with 9 steps

1: 92 percent / pyridine / 1 h

2: Et₃N / 4-dimethylaminopyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: 1.) Me₃N; 2.) NH₃ / CH₂Cl₂ / 1.) 0 deg C; 2.) 5 h, reflux

4: pyridine / 1 h

5: 1.4 g / 1 N NaOH / pyridine; H₂O / 0.17 h / 0 °C

6: pyridine / 3 h

7: Et₃N, 4-dimethylaminopyridine / diethyl ether; pyridine / Ambient temperature

8: 1.6 g / tetra-n-butylammonium flouride / tetrahydrofuran / 0.5 h

9: 2.) 2,4,6-triisopropylbenzenesulfonyl chloride / 1.) N-methylimidazole / 2.) pyridine, 30 min

With dmap; sodium hydroxide; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride; ammonia; triethylamine; trimethylamine; 1-methyl-1H-imidazole; dmap; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane; water;
DOI:10.1016/0040-4020(84)85098-X

Reference yield:

: 82921-43-5
2-N-3',5'-O-triisobutyryl-6-O-(2,4,6-triisopropylbenzenesulfonyl)-2'-deoxyguanosine

: 83327-01-9
C₆₃H₆₄ClN₈O₁₆P

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) Me₃N; 2.) NH₃ / CH₂Cl₂ / 1.) 0 deg C; 2.) 5 h, reflux

2: pyridine / 1 h

3: 1.4 g / 1 N NaOH / pyridine; H₂O / 0.17 h / 0 °C

4: pyridine / 3 h

5: Et₃N, 4-dimethylaminopyridine / diethyl ether; pyridine / Ambient temperature

6: 1.6 g / tetra-n-butylammonium flouride / tetrahydrofuran / 0.5 h

7: 2.) 2,4,6-triisopropylbenzenesulfonyl chloride / 1.) N-methylimidazole / 2.) pyridine, 30 min

With dmap; sodium hydroxide; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride; ammonia; triethylamine; trimethylamine; 1-methyl-1H-imidazole; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane; water;
DOI:10.1016/0040-4020(84)85098-X