1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

Base Information

Chemical Name:1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan
CAS No.:113354-86-2
Molecular Formula:C₇₄H₈₆O₈S₂
Molecular Weight:1167.62
Hs Code.:

Synonyms:

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Chemical Property of 1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

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Technology Process of 1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

There total 6 articles about 1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 696-63-9
4-Methoxybenzenethiol

: 113354-86-2
1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Na, 2) NaOEt / 1) ethanol, 10 min, 2) 24 h, reflux

2: 96 percent / 30 percent H₂O₂ / acetic acid / 2.5 h / Heating

3: 91 percent / 48 percent HBr/propionic acid, phenol / 36 h / Heating

4: 97 percent / K₂CO₃, NaI / dimethylformamide / 18 h / 70 °C

5: 3.2 g / DMAP, triethylamine / CH₂Cl₂ / 24 h / Heating

With dmap; hydrogen bromide; dihydrogen peroxide; sodium ethanolate; sodium; potassium carbonate; propionic acid; triethylamine; sodium iodide; phenol; In dichloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 14296-16-3
1,20-dibromoeicosane

: 113354-86-2
1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Na, 2) NaOEt / 1) ethanol, 10 min, 2) 24 h, reflux

2: 96 percent / 30 percent H₂O₂ / acetic acid / 2.5 h / Heating

3: 91 percent / 48 percent HBr/propionic acid, phenol / 36 h / Heating

4: 97 percent / K₂CO₃, NaI / dimethylformamide / 18 h / 70 °C

5: 3.2 g / DMAP, triethylamine / CH₂Cl₂ / 24 h / Heating

With dmap; hydrogen bromide; dihydrogen peroxide; sodium ethanolate; sodium; potassium carbonate; propionic acid; triethylamine; sodium iodide; phenol; In dichloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 113354-82-8
1,20-Bis(4-methoxyphenylthio)icosan

: 113354-86-2
1,20-Bis<4-<(2-triphenylmethoxy)ethoxy>phenylsulfonyl>icosan

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 30 percent H₂O₂ / acetic acid / 2.5 h / Heating

2: 91 percent / 48 percent HBr/propionic acid, phenol / 36 h / Heating

3: 97 percent / K₂CO₃, NaI / dimethylformamide / 18 h / 70 °C

4: 3.2 g / DMAP, triethylamine / CH₂Cl₂ / 24 h / Heating

With dmap; hydrogen bromide; dihydrogen peroxide; potassium carbonate; propionic acid; triethylamine; sodium iodide; phenol; In dichloromethane; acetic acid; N,N-dimethyl-formamide;