[Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆

Base Information

Chemical Name:[Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆
CAS No.:1000314-09-9
Molecular Formula:C₃₆H₃₆N₂PPt*F₆P
Molecular Weight:867.713
Hs Code.:

[Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF<sub>6</sub>

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Chemical Property of [Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆

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Technology Process of [Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆

There total 1 articles about [Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.2%

: 26042-63-7
silver(I) hexafluorophosphate

: 119743-70-3
[PtCl(Me)(2,9-dimethyl-1,10-phenanthroline)]

: 6163-58-2
tris-(o-tolyl)phosphine

: 1000314-09-9
[Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆

Guidance literature:: In methanol; dichloromethane; acetone; byproducts: AgCl; under N2 atm. to Pt complex in CH2Cl2 containing MeOH soln. AgPF6 in acetone was added, soln. was filtered, P(o-tolyl)3 was added; solvent was evapd. in vacuo, residue was crystd. from CH2Cl2-Et2O; elem.anal.;
DOI:10.1021/ic701396j

Reference yield: 81.2%

: 1000314-09-9
[Pt(Me)(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)3)]PF₆

: 1000314-15-7
[Pt(2,9-dimethyl-1,10-phenanthroline)(P(o-tolyl)2-Ph-CH2-κC,P)]PF6

Guidance literature:: In further solvent(s); soln. Pt complex in tetrachloroethane was heated at 360 K for a few hours; solvent was removed in vacuo, residue was dissolved in CH2Cl2, Et2O was added and cooled; elem. anal.;
DOI:10.1021/ic701396j