(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

Base Information

Chemical Name:(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine
CAS No.:97135-18-7
Molecular Formula:C₂₁H₁₅NO₂
Molecular Weight:313.356
Hs Code.:

(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzy<a,h>acridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

Chemical Property:

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Technology Process of (+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

There total 14 articles about (+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 97149-85-4
trans-10,11-diacetoxy-10,11-dihydrodibenz(a,h)acridine

: 97135-18-7,110927-22-5
(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; for 2.5h; Ambient temperature;
DOI:10.1021/jo00217a011

Reference yield: 25.0%

: 132297-87-1
10,11-dioxo-10,11-dihydrodibenzacridine

: 97135-18-7,110927-22-5
(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 25 ℃; for 48h;
DOI:10.1021/jo00006a063

Reference yield:

: 72019-91-1
1-chloro-6-methoxy-3,4-dihydro-2-naphthalenecarbaldehyde

: 97135-18-7,110927-22-5
(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

Guidance literature:: Multi-step reaction with 6 steps

1: 81.5 percent / 2 N HCl / ethanol / 3 h / Ambient temperature

2: 61 percent / 225 - 230 °C

3: 100 percent / 10 percent Pd-C / various solvent(s) / Heating

4: 92 percent / C₂H₅SNa / dimethylformamide / 7 h / Heating

5: 97 percent / aq. Fremy's salt / hexamethylphosphoric acid triamide / 0.16 M KH₂PO₄; 1.) 5-7 deg C, 2-2.5 h, 2.) 0 deg C, overnight

6: 25 percent / sodium borohydride / ethanol / 48 h / 25 °C

With hydrogenchloride; sodium tetrahydroborate; potassiuim nitrosodisulfonate; sodium thioethylate; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00006a063