2-nitrobenzyl diethylcarbamate

Base Information

• Chemical Name: 2-nitrobenzyl diethylcarbamate
• CAS No.: 1400301-97-4
• Molecular Formula: C₁₂H₁₆N₂O₄
• Molecular Weight: 252.27
• Mol file: 1400301-97-4.mol

Synonyms:

Chemical Property of 2-nitrobenzyl diethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-nitrobenzyl diethylcarbamate

There total 2 articles about 2-nitrobenzyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-nitrobenzyl bis(trimethoxysilylpropyl)carbamate (1384242-97-0) + diethylamine (109-89-7) → 2-nitrobenzyl diethylcarbamate (1400301-97-4)

Guidance literature:

In tetrahydrofuran; Inert atmosphere; Cooling with ice;

DOI:10.1021/ja303118w

Reference yield:

2-Nitrobenzyl alcohol (612-25-9) → 2-nitrobenzyl diethylcarbamate (1400301-97-4)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran; toluene / 40 h / 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran; hexane / -12 - 20 °C / Inert atmosphere

3: tetrahydrofuran / Inert atmosphere; Cooling with ice

With triethylamine; In tetrahydrofuran; hexane; toluene;

DOI:10.1021/ja303118w

upstream raw materials:

2-nitrobenzyl bis(trimethoxysilylpropyl)carbamate

diethylamine

2-Nitrobenzyl alcohol