9-cis-9,10-epoxyretinoic acid

Base Information

• Chemical Name: 9-cis-9,10-epoxyretinoic acid
• CAS No.: 129520-13-4
• Molecular Formula: C₂₀H₂₈O₃
• Molecular Weight: 316.441

Synonyms:

Chemical Property of 9-cis-9,10-epoxyretinoic acid

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 9-cis-9,10-epoxyretinoic acid

There total 2 articles about 9-cis-9,10-epoxyretinoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

all-trans-retinoic-acid (302-79-4) → 5,6-dihydro-5,6-dihydroxyretinoic acid (73341-58-9,102491-35-0) + trans-5,8-epoxy-5,8-dihydroretinoic acid (3012-76-8,112018-12-9,129520-10-1,129520-11-2) + cis-5,8-epoxy-5,8-dihydroretinoic acid (3012-76-8,112018-12-9,129520-10-1,129520-11-2) + 9-trans-9,10-epoxyretinoic acid (129454-98-4,129520-13-4)

Guidance literature:

With air; In ethanol; water; at 25 ℃; for 2160h; under 760 Torr; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1016/S0040-4020(01)85785-9

Reference yield:

all-trans-retinoic-acid (302-79-4) → 5,6-dihydro-5,6-dihydroxyretinoic acid (73341-58-9,102491-35-0) + trans-5,8-epoxy-5,8-dihydroretinoic acid (3012-76-8,112018-12-9,129520-10-1,129520-11-2) + cis-5,8-epoxy-5,8-dihydroretinoic acid (3012-76-8,112018-12-9,129520-10-1,129520-11-2) + 9-cis-9,10-epoxyretinoic acid (129454-98-4,129520-13-4)

Guidance literature:

With air; In ethanol; water; at 25 ℃; for 2160h; under 760 Torr; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1016/S0040-4020(01)85785-9

upstream raw materials:

all-trans-retinoic-acid

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