Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate

Base Information

• Chemical Name: Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate
• CAS No.: 84423-48-3
• Molecular Formula: C₃₆H₂₇N₂O₁₀S*Na
• Molecular Weight: 702.674
• Mol file: 84423-48-3.mol

Synonyms:

Chemical Property of Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate

There total 5 articles about Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

sodium sulfanilate (515-74-2) + 4-[4a-Methoxy-7-(4-methoxy-3,6-dioxo-cyclohexa-1,4-dienyl)-5,8-dioxo-4-phenyl-4a,5,8,8a-tetrahydro-4H-quinolin-1-yl]-benzoic acid (84410-20-8) → Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate (84423-48-3)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; water; for 8h; Heating;

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate (84423-48-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / piperidine / ethanol / 5 h / Heating

2: 80 percent / dioxane / 12 h / Heating

3: 83 percent / sodium bicarbonate / H₂O; ethanol / 8 h / Heating

With sodium hydrogencarbonate; piperidine; In 1,4-dioxane; ethanol; water;

Reference yield:

3-phenyl-propenal (104-55-2) → Sodium; 4-[1-(4-carboxy-phenyl)-9-hydroxy-4a,8-dimethoxy-5,11-dioxo-4-phenyl-1,4,4a,5,11,11a-hexahydro-pyrido[3,2-b]carbazol-6-yl]-benzenesulfonate (84423-48-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / piperidine / ethanol / 5 h / Heating

2: 80 percent / dioxane / 12 h / Heating

3: 83 percent / sodium bicarbonate / H₂O; ethanol / 8 h / Heating

With sodium hydrogencarbonate; piperidine; In 1,4-dioxane; ethanol; water;

upstream raw materials:

sodium sulfanilate

4-[4a-Methoxy-7-(4-methoxy-3,6-dioxo-cyclohexa-1,4-dienyl)-5,8-dioxo-4-phenyl-4a,5,8,8a-tetrahydro-4H-quinolin-1-yl]-benzoic acid

4,4'-Dimethoxybiphenyl-2,5,2',5'-bis-p-benzoquinone

4-(3-phenylallylideneamino)benzoic acid