N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

Base Information

Chemical Name:N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate
CAS No.:114218-48-3
Molecular Formula:C₃₀H₂₅N₆O₆PS
Molecular Weight:628.605
Hs Code.:

N<sup>6</sup>-benzoyl-O<sup>2'</sup>-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

Synonyms:

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Chemical Property of N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

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Technology Process of N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

There total 10 articles about N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69320-80-5
o-chlorophenyl N-phenylphosphoramido chloridate

: 114218-48-3
N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / 1,2,4-triazole / acetonitrile / 96 h

2: 1.) 80percent acetic acid / 1.) water, room temp., 2 d; 2.) methanol, 24 h

3: 24 percent / potassium t-butoxide / dimethylsulfoxide / 72 h / Ambient temperature

4: 32 percent / pyridine / 2 h / Ambient temperature; 1.) 0 deg C

5: 68.1 percent / 2M NaOH / ethanol; H₂O / 5 h

6: 2.) hydrogen sulphide / 1.) methylene dichloride, 12 h; 2.) pyridine, 10 min

With 1,2,4-Triazole; sodium hydroxide; hydrogen sulfide; potassium tert-butylate; acetic acid; In pyridine; ethanol; water; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 71960-50-4,71971-98-7
2',3'-ethoxymethylenadenosine 5'-

: 114218-48-3
N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 80percent acetic acid / 1.) water, room temp., 2 d; 2.) methanol, 24 h

2: 24 percent / potassium t-butoxide / dimethylsulfoxide / 72 h / Ambient temperature

3: 32 percent / pyridine / 2 h / Ambient temperature; 1.) 0 deg C

4: 68.1 percent / 2M NaOH / ethanol; H₂O / 5 h

5: 2.) hydrogen sulphide / 1.) methylene dichloride, 12 h; 2.) pyridine, 10 min

With sodium hydroxide; hydrogen sulfide; potassium tert-butylate; acetic acid; In pyridine; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 71960-51-5,71960-52-6
adenosine 5'-

: 114218-48-3
N⁶-benzoyl-O^2'-thiobenzoyladenosine cyclic 3',5'-phosphoranilidate

Guidance literature:: Multi-step reaction with 4 steps

1: 24 percent / potassium t-butoxide / dimethylsulfoxide / 72 h / Ambient temperature

2: 32 percent / pyridine / 2 h / Ambient temperature; 1.) 0 deg C

3: 68.1 percent / 2M NaOH / ethanol; H₂O / 5 h

4: 2.) hydrogen sulphide / 1.) methylene dichloride, 12 h; 2.) pyridine, 10 min

With sodium hydroxide; hydrogen sulfide; potassium tert-butylate; In pyridine; ethanol; water; dimethyl sulfoxide;