(E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

Base Information

Chemical Name:(E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene
CAS No.:205177-04-4
Molecular Formula:C₇₂H₁₄₀Ge₂Si₁₂
Molecular Weight:1488.11
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

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Technology Process of (E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

There total 1 articles about (E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 142573-07-7
{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}(mesityl)germanium dichloride

: 205177-04-4
(E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

Guidance literature:: With lithium naphthalenide; In tetrahydrofuran; (Ar), treated with lithium naphthalenide at -78°C, warmed to roomtemp.; evapd., pptd.(hexane), sublimated.(vac.) at 60°C for 3 h, washed (hexane), elem. anal.;
DOI:10.1016/S0277-5387(01)01035-X

Reference yield: 70.0%

: 617-86-7
triethylsilane

: 205177-04-4
(E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

: 157220-71-8
(C₆H₂(CH(Si(CH₃)3)2)3)(C₆H₂(CH₃)3)Ge(Si(C₂H₅)3)H

Guidance literature:: In tetrahydrofuran; (Ar), mixed at room temp., stirred overnight; evapd., chromy.(SiO2-hexane), elem. anal.;
DOI:10.1016/S0277-5387(01)01035-X

Reference yield: 62.0%

: 205177-04-4
(E)-1,2-dimesityl-1,2-bis[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]digermene

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 157220-70-7
[C₆H₂[CH(Si(CH₃)3)2]3][C₆H₂(CH₃)3]GeC₄H₄(CH₃)2

Guidance literature:: In tetrahydrofuran; (Ar), mixed at -100°C, warmed to room temp; evapd., chromy.(SiO2-hexane), elem. anal.;
DOI:10.1016/S0277-5387(01)01035-X