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Technology Process of Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6

Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6

Base Information
  • Chemical Name:Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6
  • CAS No.:148861-29-4
  • Molecular Formula:C27H24N4O3Re*F6P
  • Molecular Weight:783.684
  • Hs Code.:
Re(C<sub>5</sub>NH<sub>4</sub>C<sub>5</sub>NH<sub>4</sub>)(CO)3(C<sub>5</sub>NH<sub>4</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(CH<sub>3</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(Re(C<sub>10</sub>N<sub>2</sub>H<sub>8</sub>)(CO)3(C<sub>14</sub>N<sub>2</sub>H<sub>16</sub>))PF<sub>6</sub>

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Chemical Property of Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6
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Technology Process of Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6

There total 1 articles about Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver(I) hexafluorophosphate
26042-63-7

silver(I) hexafluorophosphate

tricarbonyl(2,2'-bipyridine)chlororhenium(I)
55658-96-3

tricarbonyl(2,2'-bipyridine)chlororhenium(I)

p-<(4-pyridyl)methyl>-N,N-dimethylaniline
131416-55-2

p-<(4-pyridyl)methyl>-N,N-dimethylaniline

Re(C<sub>5</sub>NH<sub>4</sub>C<sub>5</sub>NH<sub>4</sub>)(CO)3(C<sub>5</sub>NH<sub>4</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N(CH<sub>3</sub>)2)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(Re(C<sub>10</sub>N<sub>2</sub>H<sub>8</sub>)(CO)3(C<sub>14</sub>N<sub>2</sub>H<sub>16</sub>))PF<sub>6</sub>
148861-29-4

Re(C5NH4C5NH4)(CO)3(C5NH4CH2C6H4N(CH3)2)(1+)*PF6(1-)=(Re(C10N2H8)(CO)3(C14N2H16))PF6

Guidance literature:
In N,N-dimethyl-formamide; the Re-complex, AgPF6 and the ligand were dissolved in DMF under Ar, heated to 75°C for 2-3 h; filtered, evapd. under reduced pressure, chromy. on alumina;
DOI:10.1021/ja00066a037
upstream raw materials:

silver(I) hexafluorophosphate

tricarbonyl(2,2'-bipyridine)chlororhenium(I)

p-<(4-pyridyl)methyl>-N,N-dimethylaniline

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