Benzene, 4-heptyl-1,2-dimethoxy

Base Information

• Chemical Name: Benzene, 4-heptyl-1,2-dimethoxy
• CAS No.: 131568-28-0
• Molecular Formula: C15H24O2
• Molecular Weight: 236.354
• Mol file: 131568-28-0.mol

Synonyms:

Chemical Property of Benzene, 4-heptyl-1,2-dimethoxy

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, 4-heptyl-1,2-dimethoxy

There total 9 articles about Benzene, 4-heptyl-1,2-dimethoxy which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-(3,4-Dimethoxy-phenyl)-heptan-1-ol (64961-11-1) → 4-heptyl-1,2-dimethoxybenzene (131568-28-0)

Guidance literature:

With iron(III) chloride; In 1,2-dichloro-ethane; at 20 ℃; for 1h; chemoselective reaction;

DOI:10.1055/s-0031-1289857

Reference yield: 75.0%

1,2-dimethoxybenzene (91-16-7) + n-heptyl phenyl selenide (76376-91-5) → 4-heptyl-1,2-dimethoxybenzene (131568-28-0)

Guidance literature:

With 9,10-dimethoxyanthracene; In acetonitrile; at 20 ℃; Inert atmosphere; Irradiation;

DOI:10.1039/c7cc07529d

Reference yield: 10.0%

1-(3,4-dimethoxy-phenyl)-heptan-1-one (101100-86-1) → 4-heptyl-1,2-dimethoxybenzene (131568-28-0)

Guidance literature:

With hydrogenchloride; zinc; In toluene; for 72h; Heating;

DOI:10.1002/ejoc.200300174

upstream raw materials:

1-(3,4-dimethoxy-phenyl)-heptan-1-one

1,2-dimethoxybenzene

oenanthic acid

Heptanoic acid chloride

Downstream raw materials:

4-heptyl-pyrocatechol

2-heptyl-4,5-dimethoxy-benzaldehyde

1-(2-heptyl-4,5-dimethoxy-phenyl)-ethanone