[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)

Base Information

• Chemical Name: [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)
• CAS No.: 55998-67-9
• Molecular Formula: C₂₆H₂₆N₂NiO₄
• Molecular Weight: 489.193

Synonyms:

Chemical Property of [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)

There total 1 articles about [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone (58894-69-2) + nickel(II) acetate tetrahydrate (6018-89-9) → [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-N(6)N(9)O(3)O(12)]nickel(II) (55998-67-9)

Guidance literature:

In water; acetone; dropwise addn. of hot aq. Ni(OAc)2 to ligand (in hot Me2CO), boiling for5 min, cooling (during 2 h); concn. (reduced pressure) to crystn., dissoln. on addn. of hot Me2CO, crystn., collection (filtration), drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002101

Reference yield: 80.0%

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-N(6)N(9)O(3)O(12)]nickel(II) (55998-67-9) + uranyl(VI) acetate dihydrate → [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(4-)-N(6)N(9)O(3)O(12);O(1)O(3)O(12)O(14)]nickel(II)dioxouranium(VI) * EtOH

Guidance literature:

With ethanol; In ethanol; acetone; addn. of monometallic complex (in hot Me2CO) to metal acetate (in EtOH),warming on steam-bath for 5 min; pptn. on cooling, collection (filtration), drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002109

Reference yield: 80.0%

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-N(6)N(9)O(3)O(12)]nickel(II) (55998-67-9) + zinc(II) acetate dihydrate (5970-45-6) → [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(4-)-N(6)N(9)O(3)O(12);O(1)O(3)O(12)O(14)]nickel(II)zinc(II)hydrate (60117-00-2)

Guidance literature:

In ethanol; acetone; addn. of monometallic complex (in hot Me2CO) to metal acetate (in EtOH),warming on steam-bath for 5 min; pptn. on cooling, collection (filtration), drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002109

upstream raw materials:

5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone

nickel(II) acetate tetrahydrate

Downstream raw materials:

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)oxovanadium(IV)

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)copper(II)

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