5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone

Base Information

• Chemical Name: 5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone
• CAS No.: 58894-69-2
• Molecular Formula: C₂₆H₂₈N₂O₄
• Molecular Weight: 432.519
• Mol file: 58894-69-2.mol

Synonyms:

Chemical Property of 5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone

There total 1 articles about 5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 5-{(E)-2-[1-Methyl-3,5-dioxo-5-phenyl-pent-(E)-ylideneamino]-ethylimino}-1-phenyl-hexane-1,3-dione (58894-69-2)

Guidance literature:

1-Phenyl-1,3,5-hexantrion, Ethylendiamin;

DOI:10.1021/ja00843a065

Reference yield: 80.0%

5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone (58894-69-2) + copper(II) acetate monohydrate (6046-93-1) → [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-O(1)O(3)O(12)O(14)]copper(II) hydrate

Guidance literature:

In ethanol; chloroform; addn. of hot soln. of ligand (in CHCl3) to hot soln. of metal salt (in EtOH), warming on steam-bath for 5 min (dissoln.); crystn. on cooling, collection (filtration), drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002101

Reference yield: 70.0%

5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraone (58894-69-2) + uranyl(VI) acetate dihydrate → [UO2(5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-O(1)O(3)O(12)O(14))] * EtOH e

Guidance literature:

With ethanol; In ethanol; chloroform; addn. of ligand (in CHCl3) to UO2(OAc)2 (in hot EtOH), warming on steam-bath for 5 min; pptn. on cooling, collection (filtration), washing by boiling in EtOH, drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002101

Downstream raw materials:

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]dicopper(II)

PdUO₂(C₂₆H₂₄N₂O₄)*H₂O