acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique

Base Information

• Chemical Name: acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique
• CAS No.: 73739-68-1
• Molecular Formula: C₁₂H₂₀O₃
• Molecular Weight: 212.289
• Mol file: 73739-68-1.mol

Synonyms:

Chemical Property of acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique

There total 16 articles about acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-3,4-dihydro-2H-pyran (4454-05-1) → acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique (73739-68-1,73739-69-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 2.) sodium hydroxide / 1.) xylene, reflux, 4 d, 2.) water, methanol, reflux, 7 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex; In methanol; water; acetic acid;

Reference yield:

2-methoxy-3,4-dihydro-2H-pyran (4454-05-1) → acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique (73739-68-1,73739-69-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 2.) sodium hydroxide / 1.) xylene, reflux, 4 d, 2.) water, methanol, reflux, 7 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex; In methanol; water; acetic acid;

Reference yield:

1,1,5,5-tetramethoxy-pentane (4454-02-8) → acide methoxy-5 methylene-2 dimethyl-6,6 cyclohexane acetique (73739-68-1,73739-69-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 61 percent / boron trifluoride etherate / Ambient temperature

2: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

3: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

4: 2.) sodium hydroxide / 1.) xylene, reflux, 4 d, 2.) water, methanol, reflux, 7 h

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; In methanol; water; acetic acid;

upstream raw materials:

N,N-dimethylacetamide dimethyl acetal

hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

(methoxy-4 dimethyl-3,3 cyclohexene-1 ylmethyl) vinylether

Triethyl orthoacetate